3-(pyridin-2-yl)-1,2,4-triazole was synthesized through two steps from the raw material 2-cyanopridine,and a series of derivatives(3a～3d)which were reported in this paper were synthesized by the reaction of 3-(pyridin-2-yl)-1,2,4-triazole with(o-,m-,p-)2-chloro-methyl pyridine.Their structures were characterized by elementary analyses,IR,1H NMR and 13C NMR.
