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杨跃

作品数:4 被引量:10H指数:2
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槲皮素-3’-氨基酸酯盐酸盐的合成工艺研究被引量:4
2008年
The synthetic route of 3’-amino carboxylate hydrochloride of quercetin is improved.Using benzyl bromide to partly protect the hydroxyl groups,the protected quercetin then react with a series of Boc protected amino acids to afford the 3’-amino carboxylate,hydrogenised and treated with HCl(g),a series of 3’-amino carboxylate hydrochloride of quercetin are synthesized in good yields.The structures of these compounds are confirmed by means of their m.p.,mass spectra and 1H NMR.
于姝燕杨跃郑永胜郭举吴成龙罗娟田之悦成丽
关键词:槲皮素
微波辐射在合成沙利度胺的铵盐类衍生物中的应用
2009年
Amino acid benzyl ester p-toluenesulfonic acids were synthesized under microwave irradiation condition by reaction of four amino acids with benzyl alcohol and p-toluenesulfonic acid,and then reacted with the N-phthaloyl-L-glutamic anhydride to yield compound 3a-d,hydrogenised and treated with NH3(g) to obtain the target compounds—thalidomide ammonium salt derivatives.The microwave-assisted method was used to synthesis the thalidomide amino acid benzyl ester p-tolunensulfonic acid,the reaction time was brought down with improved yield as compared with conventional heating method.The structures were comfirmed by MS,1H-NMR and elemental analysis.
郭举郑永胜郭栋汪宏于姝燕杨跃田之悦罗娟成丽
关键词:微波辐射
1,3-二氢-1,3-二酮-2-氢-异吲哚衍生物的合成研究被引量:1
2008年
目的设计并合成沙利度胺的衍生物。方法氨基酸苄酯氨解N-邻苯二甲酰基-L-谷氨酸酐,所得产物经氢化脱苄后再与氨气成铵盐即得1,3-二氢-1,3-二酮-2H-异吲哚衍生物。结果成功地合成了4个未见文献报道的沙利度胺衍生物。并进行了结构表征。结论利用本方法可以在温和的条件下获得较高产率的目标产物。
杨跃向东郭举郑永胜叶斌杨金亮成丽
关键词:沙利度胺血管生成
1-(3-甲基-1-氨基)丁烷基硼酸频哪醇酯盐酸盐的合成研究被引量:5
2008年
The hydrochloride of 1-(1-amino-3-methyl)butyl borate pinacol is prepared by using the isobutylbromide to form the Grignard agent.The product is protected with the pinacol,then reacted with the lithium diisopropylamide and the anhydrous zinc chloride.Finally,the product is synthesized in the existence of the LHMDS.All the compounds are confirmed by MS and 1H-NMR.
郑永胜郭举陈丹李峰杨跃于姝燕田之悦罗娟成丽
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