Chitosan-TiO2 composite has been prepared by the sol-gel process. Tetrabutyl titanate( TTB) was used as a precursor to obtain nano TiO2 sol,which was then added into acid solution of chitosan to form titania network in the matrix. SEM,TG,and Fourier transform infrared spectroscopy( FTIR) were employed to characterize morphology and structure of the Chitosan-TiO2 composite. The resulting hybrid has potential applications for the adsorption and sonolytic-degradation of organic dyes in wastewater.The result shows that the de-coloring ratio reaches 97. 2% at the optimum conditions with the help of ultrasound.