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国家自然科学基金(51271035)

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29 条 记 录,以下是 1-10
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低碳铁素体钢中纳米尺寸碳化物的相间析出特征被引量:5
2014年
分别在600、650和700℃度对Ti-Mo低碳钢进行等温处理,对其力学性能进行检测并利用扫描电镜观察其显微组织,最后通过透射电镜和选区电子衍射对纳米尺寸碳化物的相间析出特征进行研究分析。结果表明:相间析出的排间距随着处理温度的降低而减小;排间距的平均值是常量,但单个排间距的值变化很大,两个特定行之间的排间距变化不大;不同方向析出的相间析出粒子之间存在着竞争关系,当两方相遇时,其中某一方向或被迫中断,或发生偏转直至两者的方向几乎相同,这是形成不同的相间析出台阶高度的一个原因;相间析出粒子的析出面并非只固定在{110}α面上,相间析出也可以在铁素体的其他晶面上发生。
汪小培赵爱民赵征志黄耀何建国赵复庆
关键词:等温温度
Microstructure and Mechanical Properties of NANOBAIN Steel
2016年
The microstructure and mechanical properties of NANOBAIN steel treated at different isothermal temperatures were investigated by scanning electron microscopy(SEM),transmission electron microscopy(TEM),uniaxial tensile tests and X-ray diffraction(XRD).It was found that bainitic ferrite(BF)plate was made of basic shear transformation units arranged in the same direction of subunits.The existence of defects,such as nanoscale twinning and dislocation,suggested that the growth of transformation units was controlled by the surrounding defect plane with dislocation,which was consistent with the moving direction of BF/austenite interface parallel to the twinning plane.The behavior of work hardening indicated that mechanical stability of microstructures obtained at 250 ℃ and 300 ℃ was much more stable than that obtained at 210℃.The evolution of carbon partitioning in retained austenite and bainitic ferrite also indicated that austenite was enriched in carbon at the initial stage step by step;after the formation of BF,the austenite did not seem to be greatly enriched in carbon and the carbon content showed a little decrease instead;subsequently,aphenomenon of little decarburization of supersaturated bainitic ferrite has also been found.
Yao HUANGXue-li ZHANGWei-ning LIUXu-min WANGJun-ke HAN
Effects of Mn and Cr contents on microstructures and mechanical properties of low temperature bainitic steel被引量:3
2017年
The effects of Mn and Cr contents on bainitic transformation kinetics,microstructures and mechanical properties of high-carbon low alloy steels after austempered at 230,300 and 350 ℃ were determined by dilatometry,optical microscopy,scanning electron microscopy,X-ray diffraction and tensile tests. The results showed that Mn and Cr can extend bainitic incubation period and completion time,and with the increase of Mn and Cr content,the bainitic ferrite plate thickness decreased and the volume fraction of retained austenite increased. TRIP( transformation induced plasticity) effect was observed during tensile testing which improved the overall mechanical property. The increase of Mn concentration can improve the strength to a certain extent,but reduce the ductility. The increase of Cr concentration can improve the ductility of bainitic steels which transformed at a low temperature. The low temperature bainitic steel austempered at 230 ℃ exhibited excellent mechanical properties with ultimate tensile strength of( 2146 ± 11) MPa and total elongation of( 12. 95 ± 0. 15) %.
Hui GuoPeng ZhouAi-min ZhaoChao ZhiRan DingJia-xing Wang
关键词:贝氏体钢钢组织铬含量扫描电子显微镜高碳低合金钢X射线衍射仪
加热温度对超纯铁素体含铜不锈钢热脆敏感性的影响
2015年
在Gleeble-3500热模拟机上对21Cr-1.4Cu超纯铁素体不锈钢进行高温拉伸试验,研究加热温度对试验钢热脆敏感性的影响。采用扫描电子显微镜、激光共聚焦显微镜和能谱分析等方法对显微组织和化学成分进行了对比分析。结果表明,1300℃加热时,试验钢由于过烧产生了高温脆性。1150℃加热时,热脆敏感性最高,产生铜裂。1200~1250℃加热时,热脆敏感性较低,发生塑性变形。研究发现,加热温度为1150℃时,形成的氧化物开始呈液态,冷却后形成包裹状或共晶结构的硅酸盐细颗粒。这些脆性物质使晶界强度降低,结合松脆最后导致严重铜裂。
尹鸿祥赵爱民赵征志周开春裴伟梁江涛
关键词:热脆性高温变形铁素体不锈钢
马氏体基TRIP钢的组织与力学性能
2014年
在基本C-Si-Mn系TRIP钢的基础上,通过调整工艺参数获得具有马氏体基的TRIP钢,通过扫描电镜分析、透射电镜分析、电子背散射衍射分析、X射线衍射分析、单向拉伸实验等对经不同工艺处理的实验用钢的显微组织和力学性能进行了对比分析.结果表明:两相区退火温度升高,铁素体比例减少,贝氏体比例增加,残余奥氏体整体先增加后减少;在较低温度下退火时,条状铁素体合并成为块状铁素体;在较高温度下退火时,条状奥氏体合并成为块状奥氏体,随后在冷却过程中转变为马氏体或残余奥氏体;实验钢在780℃退火时,获得最佳综合力学性能,此时抗拉强度达1053MPa,延伸率达23%,强塑积达24GPa×%.一定量的细小弥散的板条残余奥氏体是实验钢获得高强塑积的主要原因.
尹鸿祥赵爱民赵征志庞启航何建国张聪
关键词:TRIP钢马氏体残余奥氏体力学性能
Mo含量对Ti微合金低碳钢力学性能的影响被引量:2
2014年
对Ti微合金钢和不同Mo/Ti原子配比的Ti-Mo合金钢进行组织观察和力学性能分析,并利用透射电镜对钢中析出的纳米级的碳化物粒子的形貌分布进行分析。结果表明,在Ti微合金钢中添加Mo能够使钢的强度显著提高;在Ti含量一定的条件下,随着Mo的增加,钢的屈服强度和抗拉强度呈先增大后减小趋势;Mo/Ti的原子比值分别为0.7、1.1和1.3时,钢的力学性能在原子比值为1.1时最优,其抗拉强度达825 MPa。
汪小培赵征志赵爱民耿志达
关键词:力学性能
低碳钢中纳米尺寸碳化物的相间析出行为被引量:4
2015年
采用扫描电镜和透射电子显微镜对低碳Ti-Mo系的热轧板进行了组织分析,同时对其中的纳米粒子析出行为进行了研究.强化机理分析表明析出强化对于屈服强度的贡献值可达291 MPa.随着卷取温度的降低,纳米粒子相间析出的排间距会减小,相间析出的排间距与其在铁素体中形核点位置有一定的离散值,但基本上呈一定的固定值.α/γ界面的观察和采用不同理论的计算结果表明相间析出的产生主要与α/γ界面的台阶形成有关,相间析出的排间距大小由台阶高度、晶界扩散系数、等温温度、台阶面迁移速率等决定.
黄耀赵爱民程永峰汪小培杨靖波刘华清
关键词:低碳钢碳化物
Effect of Annealing Process on Microstructure and Mechanical Property of 1100 MPa Grade TRIP Steel被引量:2
2015年
To develop super-high strength TRIP steel for automobile application with good combination of strength and plasticity,an ultra-high-strength TRIP steel 0.2%C-2.0%Si-1.8%Mn was investigated at different intercritical annealing temperatures and bainitic isothermal temperatures.Microstructures were observed by scanning electron microscopy,transmission electron microscopy,electron backscatter diffraction,and X-ray diffraction,and mechanical properties were tested under a uniaxial tensile testing machine.It shows that the best comprehensive mechanical properties were obtained for the experimental steel particularly annealed at 820 ℃ and austempered at 410 ℃.Yield strength of the tested steel mainly depends on ferrite,while the high strength of the tested steel is related to martensite which forms through blocky austenite transformation during cooling and subsequent tensile test attributed to the TRIP effect.Hence,it could be concluded that the grain size of the retained austenite and carbon content in retained austenite are the main reasons for high elongation of the tested steel.
Hong-xiang YINZheng-zhi ZHAOAi-min ZHAOXiao LIHan-jiang HUJiang-tao LIANG
关键词:透射电子显微镜电子背散射衍射拉伸试验机奥氏体相变
纳米贝氏体的热力学分析及强韧化研究被引量:3
2016年
针对目前高碳高硅低温贝氏体(纳米结构贝氏体)相变速度缓慢的现状,采用贝氏体相变热力学理论分析主要合金元素对低温贝氏体相变驱动力的影响,设计了新型纳米结构贝氏体钢成分0.83C-2.44Si-0.43Mn-0.73Al.利用膨胀仪研究该成分贝氏体钢在不同温度下的相变整体动力学,综合使用扫描电子显微镜、X射线衍射、电子背散射衍射等方法研究热处理工艺对实验钢组织和力学性能的影响.结果表明,350℃等温转变贝氏体的抗拉强度为1401 MPa,延伸率为42.21%,强塑积可达59136 MPa·%,在室温拉伸过程中发生明显的相变诱导塑性效应;230℃等温转变组织中贝氏体铁素体片层厚度小于100 nm,抗拉强度达2169 MPa.
智超赵爱民何建国赵复庆车英建
关键词:贝氏体钢纳米结构材料热力学分析
Mechanical properties and characteristics of nanometer-sized precipitates in hot-rolled low-carbon ferritic steel被引量:9
2014年
The microstructures and properties of hot-rolled low-carbon ferritic steel have been investigated by optical microscopy, field-emission scanning electron microscopy, transmission electron microscopy, and tensile tests after isothermal transformation from 600°C to 700°C for 60 min. It is found that the strength of the steel decreases with the increment of isothermal temperature, whereas the hole expansion ratio and the fraction of high-angle grain boundaries increase. A large amount of nanometer-sized carbides were homogeneously distributed throughout the material, and fine(Ti, Mo)C precipitates have a significant precipitation strengthening effect on the ferrite phase because of their high density. The nanometer-sized carbides have a lattice parameter of 0.411-0.431 nm. After isothermal transformation at 650°C for 60 min, the ferrite phase can be strengthened above 300 MPa by precipitation strengthening according to the Ashby-Orowan mechanism.
Xiao-pei WangAi-min ZhaoZheng-zhi ZhaoYao HuangLiang LiQing He
关键词:纳米尺寸铁素体钢析出物场发射扫描电子显微镜
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